Fabrication of Nanohydroxyapatite-Chitosan Coatings by Pulse Electrodeposition Method

نویسندگان

چکیده

In this study, Mg–2 wt% Zn scaffolds were fabricated by the powder metallurgy method, and effects of porosity content on microstructure, mechanical properties studied. Nanocomposite coatings deposited pulse electrodeposition (PED) method Mg–2Zn studied using a scanning electron microscope (SEM), X-ray diffraction (XRD), energy-dispersion spectrometer (EDS), Fourier transform infrared spectroscopy (FT-IR). The morphologies showed that optimal coating was obtained at 40 V voltages, 10 min time nanohydroxyapatite(nHA)/chitosan (CS) ratio = 10. pulse-peak current density (CD), duty cycles (DC), pH temperature considered mA/cm2, 0.2,7 37 °C, respectively. coating, Ca/P atomic 1.57, which is similar to value bone hydroxyapatite. corrosion resistance thermal stability examined potentiodynamic polarization thermogravimetric analysis (TGA), results rate 0.58 mm/year, very low appropriate in compared with 2.09 mm/year. TGA indicated significant weight loss about 23% 14% for CS vitro biocompatibility evaluated cell adhesion, cytotoxicity, alkaline phosphatase (ALP) assays MG63 cells. indicate nanocomposite highly biocompatible, making material more suitable applications tissue engineering repair defects caused sports injuries.

برای دانلود باید عضویت طلایی داشته باشید

برای دانلود متن کامل این مقاله و بیش از 32 میلیون مقاله دیگر ابتدا ثبت نام کنید

اگر عضو سایت هستید لطفا وارد حساب کاربری خود شوید

منابع مشابه

Preparation of Gd2O3 Ultrafine Nanoparticles by Pulse Electrodeposition Followed by Heat-treatment Method

Gd2O3 nanoparticles were prepared by a two–step process; cathodic electrodeposition followed by heat-treatment method. First, Gd(OH)3 nanoparticles was galvanostatically deposited from nitrate bath on the steel substrate by pulse current (PC) mode. The deposition experiments was conducted at a typical on-time and off-time (ton=1ms and toff=1ms) for 60 min. The electrodeposited precursor was the...

متن کامل

Electrodeposition of Nanostructured Magnesium Coatings

In this work, we report on the electroplating of ultrafine and uniform magnesium (Mg) films on copper (Cu) and carbon nanotube (CNT) paper substrates. By controlling the process parameters and utilizing the pulsed deposition method, the average grain size of Mg was reduced to nanodimensions. Surface pretreatment of the substrates by depositing a seed layer was found to be an efficient strategy ...

متن کامل

A Rapid One-Step Process for Fabrication of Biomimetic Superhydrophobic Surfaces by Pulse Electrodeposition

Inspired by some typical plants such as lotus leaves, superhydrophobic surfaces are commonly prepared by a combination of low surface energy materials and hierarchical micro/nano structures. In this work, superhydrophobic surfaces on copper substrates were prepared by a rapid, facile one-step pulse electrodepositing process, with different duty ratios in an electrolyte containing lanthanum chlo...

متن کامل

preparation of gd2o3 ultrafine nanoparticles by pulse electrodeposition followed by heat-treatment method

gd2o3 nanoparticles were prepared by a two–step process; cathodic electrodeposition followed by heat-treatment method. first, gd(oh)3 nanoparticles was galvanostatically deposited from nitrate bath on the steel substrate by pulse current (pc) mode. the deposition experiments was conducted at a typical on-time and off-time (ton=1ms and toff=1ms) for 60 min. the electrodeposited precursor was the...

متن کامل

Bone repair by periodontal ligament stem cellseeded nanohydroxyapatite-chitosan scaffold

BACKGROUND A nanohydroxyapatite-coated chitosan scaffold has been developed in recent years, but the effect of this composite scaffold on the viability and differentiation of periodontal ligament stem cells (PDLSCs) and bone repair is still unknown. This study explored the behavior of PDLSCs on a new nanohydroxyapatite-coated genipin-chitosan conjunction scaffold (HGCCS) in vitro as compared wi...

متن کامل

ذخیره در منابع من


  با ذخیره ی این منبع در منابع من، دسترسی به آن را برای استفاده های بعدی آسان تر کنید

ژورنال

عنوان ژورنال: Journal of Inorganic and Organometallic Polymers and Materials

سال: 2022

ISSN: ['1574-1451', '1574-1443']

DOI: https://doi.org/10.1007/s10904-022-02468-w